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It turned out he was killed by something far more lethal than common rat poison. >> it's polonium. >> polonium 210 to be exact, a rare and deadly radioactive isotope. the news shocked the world, even though most people weren't exactly sure what polonium was. but paul joyal knew what it was and what it could do. that his friend effectively burned to death from radioactivity. >> it's a horrible death. it's a gruesome death. he lived longer than he -- than any man normally would under those circumstances. and he lived just long enough, within 12 hours long enough, for them to finally determine th...

Them to finally determine that it was polonium versus something else. >> reporter: why, if he had died 12 hours earlier, would it have made any difference? >> because they wouldn't have found out. they would have marked the death certificate as death unknown. he would have been put in the ground, and it would have been just a mystery. unknown -- unknown assailants. turn the page, move on. >> it's the key of this murder. polonium 210 was discovered and now we know exactly sasha was killed by polonium 210. >> reporter: it's an almost perfect murder weapon. polonium has no smell, little taste, an...

Certificate as death unknown. he would have been put in the ground, and it would have been just a mystery. unknown -- unknown assailants. turn the page, move on. >> it's the key of this murder. polonium 210 was discovered and now we know exactly sasha was killed by polonium 210. >> reporter: it's an almost perfect murder weapon. polonium has no smell, little taste, and without specialized equipment, it's undetectable. >> reporter: the amount that killed litvinenko, slipped into something he ate or drank, was no larger than a grain of salt. but that's still a thousand times the lethal dose. and...

12 hours earlier, would it have made any difference? >> because they wouldn't have found out. they would have marked the death certificate as death unknown. he would have been put in the ground, and it would have been just a mystery. unknown -- unknown assailants. turn the page, move on. >> it's the key of this murder. polonium 210 was discovered and now we know exactly sasha was killed by polonium 210. >> reporter: it's an almost perfect murder weapon. polonium has no smell, little taste, and without specialized equipment, it's undetectable. >> reporter: the amount that killed litvinenko, sli...

>> reporter: why, if he had died 12 hours earlier, would it have made any difference? >> because they wouldn't have found out. they would have marked the death certificate as death unknown. he would have been put in the ground, and it would have been just a mystery. unknown -- unknown assailants. turn the page, move on. >> it's the key of this murder. polonium 210 was discovered and now we know exactly sasha was killed by polonium 210. >> reporter: it's an almost perfect murder weapon. polonium has no smell, little taste, and without specialized equipment, it's undetectable. >> if you not look...