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Grants from the Provost and the Dean for Research will transform materials science, synthesis, catalysis, and chemical biology research across campus through the acquisition of a powerful new Nuclear Magnetic Resonance (NMR) spectroscopy tool and an extensive facility upgrade.
Background Multidimensional solid-state nuclear magnetic resonance (ssNMR) spectroscopy has emerged as an indispensable technique for resolving polymer structure and intermolecular packing in primary and secondary plant cell walls. Isotope ( 13C) enrichment provides feasible sensitivity for measuring 2D/3D correlation spectra, but this time-consuming procedure and its associated expenses have restricted the application of ssNMR in lignocellulose analysis. Results Here, we present a method that relies on the sensitivity-enhancing technique Dynamic Nuclear Polarization (DNP) to eliminate the ne...