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Layered crystal structures of various materials form through strong in-plane covalent and weaker out-of-plane bonding. The different bonding states can lead to the appearance of anisotropies not only of electronic/electrical and magnetic properties but also of structural disorder. A deeper understanding of the disorder anisotropy is essential to carry out structural modification and to enhance the material properties. However, in the case of multi-band MgB2 superconducting materials that have layered structures, including graphene-like and six-membered rings, the nature and extent of the disor...

Powder processing by ball milling is an effective approach for materials engineering. Although various methods for material processing are available, only high-energy shaker/vibratory or planetary mills have been intensively utilized to develop mechanical milling or alloying routes for structural control of MgB2 superconducting materials. Herein, we have attempted structural modification by using a low-rotation shaker, which is categorized as a low-energy and economical mill in terms of industrial applications. The operation speed was kept constant at 40 rpm, which is much lower than typical c...