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Alumina-forming austenitic (AFA) steel, a promising candidate for use in high-temperature components of ultra-supercritical power plants, has high creep strengths and outstanding high-temperature corrosion resistance. The effects of microstructural evolution on the mechanical properties of Fe-20Ni-14Cr-3Al alumina-forming austenitic (3Al-AFA) steel with micro-cold deformation were investigated by multiple characterization methods, and the micro-cold deformation process was analyzed by conducting compression experiments. Tensile properties and hardness were also examined. The results show that the reduction of deformation has significant influences on the increase in the density of dislocation, the reduction of grain size, and the distribution of precipitates, which play an essential role in the enhancement of mechanical properties. As the reduction of deformation increases, the density of dislocations rises, the fragmentation of grains results in a reduction of grain size, and the dist
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